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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 972377Generated: October 29, 2026

Cyclohexyl isocyanate → HCID 178485086, compound

https://huagongshe.com/reaction/972377

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexyl isocyanateHCID 18502—
ReactantN,N,N′-TrimethylguanidineHCID 141619—
SolventTolueneHCID 1140—
ProductHCID 178485086HCID 178485086—

Reaction Steps

To 60.6 parts by weight of 1,1,2-trimethylguanidine in 600 parts by volume of toluene are added dropwise with cooling 75 parts by weight of cyclohexyl isocyanate. After evaporation of the solvent in vacuo, the product is recrystallized from acetonitrile to yield 2-cyclohexylcarbamoyl-1,1,3-trimethylguanidine, m.p. 121°-124° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04053299
Source datasetuspto-grants-1977_10
ORD IDord-bd00a2121e2842f294c6457713ad36d7
Source noteuspto-grants-1977_10