Methyl Thioglycolate → HCID 21404635, compound

HRID 972477Notes

Reaction equation

[CH3:1][N:2]([CH3:19])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH:13]=[N:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:20](OC)(=[O:23])[CH2:21][SH:22]>>[CH2:15]([N:14]1[C:20](=[O:23])[CH2:21][S:22][CH:13]1[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[O:6][CH2:5][CH2:4][CH2:3][N:2]([CH3:1])[CH3:19])[CH2:16][CH2:17][CH3:18]

Participants

Reactant 2

HCID 16907Methyl Thioglycolate

HCID 20394049HCID 20394049, compound

Product 1

HCID 21404635HCID 21404635, compound

Procedure

N-[[2-[3-(Dimethylamino)propoxy]phenyl]methylene]-butanamine (5.2 g) is reacted with 4.2 g of methyl thioglycolate following the procedure described in Example 1, part B, to yield 6.5 of 3-butyl-2-[2-[3-(dimethylamino)propoxy]phenyl]-4-thiazolidinone as an oil.

Sources & evidence

ORD record: ord-959ac7eddc404cd0bf1a0e4ff5d2e23d
Source dataset: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04053471

Reaction notes

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