HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54293063, compound → HCID 21404648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54293063 | HCID 54293063 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21404648 | HCID 21404648 | — |
Reaction Steps
A suspension of 10 parts of 2-[2-[3-(methylethylamino)propoxy]phenyl]-3-[2-(4-nitrophenyl)ethyl]-4-thiazolidinone (see Example 19) in 100 ml of ethanol is treated with 1 part of 5% palladium on carbon and placed under 3 atmospheres of gaseous hydrogen. The mixture is shaken until one equivalent of hydrogen is consumed, filtered and the solvent evaporated under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053471 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-b21a94b064df4707b669617d59f895bb |
| Source note | uspto-grants-1977_10 |