HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → HCID 532253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 532253 | HCID 532253 | — |
Reaction Steps
Subject 6.5 g. (33.0 mmoles) of 1-adamantane carboxylic acid chloride, 4.0 g. (33.0 mmoles) of p-anisidine and 10.0 ml. of triethylamine to the process of Example 11 and crystallize the residue obtained thereby from chloroform to yield the title product, m.p. 181°-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053509 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-9b1cc9e9176a4b8ea324953b58cf5b85 |
| Source note | uspto-grants-1977_10 |