P-Anisidine → HCID 532253, compound

HRID 972646Notes

Reaction equation

HRID 972646 reaction equation
[C:1]12([C:11](Cl)=[O:12])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH3:14][O:15][C:16]1[CH:21]=[CH:20][C:19]([NH2:22])=[CH:18][CH:17]=1>C(Cl)(Cl)Cl>[CH3:14][O:15][C:16]1[CH:21]=[CH:20][C:19]([NH:22][C:11]([C:1]23[CH2:10][CH:5]4[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]4)[CH2:2]2)[CH2:8]3)=[O:12])=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 7732P-AnisidineHCID 989151-Adamantanecarbonyl chloride

Product 1

HCID 532253HCID 532253, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Subject 6.5 g. (33.0 mmoles) of 1-adamantane carboxylic acid chloride, 4.0 g. (33.0 mmoles) of p-anisidine and 10.0 ml. of triethylamine to the process of Example 11 and crystallize the residue obtained thereby from chloroform to yield the title product, m.p. 181°-184° C.

Workup

  1. customof triethylamine to the process of Example 11 and crystallize the residue
  2. customobtained

Sources & evidence

ORD record
ord-9b1cc9e9176a4b8ea324953b58cf5b85
Source dataset
uspto-grants-1977_10
Patent number
US04053509

Reaction notes

Loading…