HuagongsheHuagongshe Chemistry Print Report · For research reference only
Homoveratrylamine → HCID 3939109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Homoveratrylamine | HCID 8421 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| Solvent | Diethylether ethylacetate | HCID 21584169 | — |
| Product | HCID 3939109 | HCID 3939109 | — |
Reaction Steps
Subject 2.0 g. of adamantane carboxylic acid chloride 1.8 g. (10.0 mmoles) of homoveratrylamine and 5.0 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from an ethyl acetate-ethyl ether mixture to obtain the title product, m.p, 132°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053509 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-6e257a50995c4f26a8ad21c3e850feb9 |
| Source note | uspto-grants-1977_10 |