Homoveratrylamine → HCID 3939109, compound

HRID 972650Notes

Reaction equation

HRID 972650 reaction equation
[C:1]12([C:11](Cl)=[O:12])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[CH2:14]([NH2:26])[CH2:15][C:16]1[CH:25]=[CH:24][C:21]([O:22][CH3:23])=[C:18]([O:19][CH3:20])[CH:17]=1.C(N(CC)CC)C>C(OCC)(=O)C.C(OCC)C>[CH3:20][O:19][C:18]1[CH:17]=[C:16]([CH2:15][CH2:14][NH:26][C:11]([C:1]23[CH2:10][CH:5]4[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]4)[CH2:2]2)[CH2:8]3)=[O:12])[CH:25]=[CH:24][C:21]=1[O:22][CH3:23]

Participants

5

Reactant 3

HCID 8421HomoveratrylamineHCID 8471TriethylamineHCID 989151-Adamantanecarbonyl chloride

Product 1

HCID 3939109HCID 3939109, compound

Reagents, catalysts & solvents 1

HCID 21584169Diethylether ethylacetateSolvent

Procedure

Subject 2.0 g. of adamantane carboxylic acid chloride 1.8 g. (10.0 mmoles) of homoveratrylamine and 5.0 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from an ethyl acetate-ethyl ether mixture to obtain the title product, m.p, 132°-133° C.

Workup

  1. customCrystallize the residue
  2. customobtained

Sources & evidence

ORD record
ord-6e257a50995c4f26a8ad21c3e850feb9
Source dataset
uspto-grants-1977_10
Patent number
US04053509

Reaction notes

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