HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 3120174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Reactant | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 3120174 | HCID 3120174 | — |
Reaction Steps
Subject 4.0 g. (29.0 mmoles) of p-methoxy-benzylamine, 5.7 g. (29.0 mmoles) of adamantane carboxylic acid chloride and 10 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from chloroform to obtain the product of this Example, m.p. 91°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053509 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-2ca0e7739857428da143a5aff21e03d9 |
| Source note | uspto-grants-1977_10 |