Triethylamine → HCID 3120174, compound

HRID 972656Notes

Reaction equation

HRID 972656 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH2:8])=[CH:5][CH:4]=1.[C:11]12([C:21](Cl)=[O:22])[CH2:20][CH:15]3[CH2:16][CH:17]([CH2:19][CH:13]([CH2:14]3)[CH2:12]1)[CH2:18]2.C(N(CC)CC)C>C(Cl)(Cl)Cl>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][NH:8][C:21]([C:11]23[CH2:20][CH:15]4[CH2:14][CH:13]([CH2:19][CH:17]([CH2:16]4)[CH2:18]2)[CH2:12]3)=[O:22])=[CH:5][CH:4]=1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 754524-MethoxybenzylamineHCID 989151-Adamantanecarbonyl chloride

Product 1

HCID 3120174HCID 3120174, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Subject 4.0 g. (29.0 mmoles) of p-methoxy-benzylamine, 5.7 g. (29.0 mmoles) of adamantane carboxylic acid chloride and 10 ml. of triethylamine to the process of Example 11. Crystallize the residue obtained thereby from chloroform to obtain the product of this Example, m.p. 91°-94° C.

Workup

  1. customCrystallize the residue
  2. customobtained

Sources & evidence

ORD record
ord-2ca0e7739857428da143a5aff21e03d9
Source dataset
uspto-grants-1977_10
Patent number
US04053509

Reaction notes

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