HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 131710936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | HCID 70631851 | HCID 70631851 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131710936 | HCID 131710936 | 10.8% |
Reaction Steps
A stirred solution of 8.6 g (0.024 mole) of 2-[[3-[3-(dimethylamino)propoxy]phenyl]methylene]-2,3-dihydro-1H-inden-1-one hydrochloride from part B and 1.3 g (0.028 mole) of methyl hydrazine in 50 ml of methanol is heated at reflux for 2 hours. After cooling, the solvent is evaporated to give 1.0 g of an amber oily residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053514 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-f01056cc0e8147c7b0418e693cb1ed3e |
| Source note | uspto-grants-1977_10 |