HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 21404528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 21404525 | HCID 21404525 | — |
| Catalyst | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 21404528 | HCID 21404528 | — |
Reaction Steps
6-[m-(Methylamino)phenyl]-1,2-dihydro-2-oxonicotinic acid (1.0 g.) is added to 10 ml. of SOCl2 containing 10 drops of dimethylformamide. Solution soon occurred, and after about 15 minutes, a new solid starts to appear. The mixture is diluted with methylene chloride, and the 6-[m-(methylamino)phenyl]-1,2-dihydro-2-oxonicotinyl chloride hydrochloride collected and washed with methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053470 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-9a66cf1b085b48d3a8818ba3f09ef986 |
| Source note | uspto-grants-1977_10 |