HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 21404571, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 21404552 | HCID 21404552 | — |
| Catalyst | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 21404571 | HCID 21404571 | — |
Reaction Steps
6-[m-(Propylamino)phenyl]-1,2-dihydro-2-oxonicotinic acid (1.0 g.) is added to 10 ml. thionyl chloride containing 10 drops of dimethylformamide. Solution soon occurs and after a half hour a new solid appears. The mixture is diluted with methylene chloride and the 6-[m-(propylamino)phenyl]-1,2-dihydro-2-oxonicotinyl chloride hydrochloride collected and washed with methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053470 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-5d53b255f26245b29ccd56581e3a854a |
| Source note | uspto-grants-1977_10 |