HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20309559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20309576 | HCID 20309576 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20309559 | HCID 20309559 | — |
Reaction Steps
Methyl 4-(3-t-butylamino-2-hydroxypropoxy)-3-(3-carbomethoxypropionyl)benzoate was heated with dilute sodium hydroxide solution until hydrolysis was complete. The solution was neutralised with acetic acid then evaporated under reduced pressure. Extraction of the residue with ethanol and evaporation of the extracts gave 4-(3-t-butylamino-2-hydroxypropoxy)-3-(3-carboxypropionyl)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053601 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-86e2f7d6e55749a6b4efd84110635a18 |
| Source note | uspto-grants-1977_10 |