Homoallyl bromide → HCID 135727401, compound
Reaction equation
[Cl:1][C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][C:9]=2[OH:15])=[CH:6][CH:7]=1.[CH2:16](Br)[CH2:17][CH:18]=[CH2:19]>>[CH2:19]([O:14][C:11]1[CH:12]=[CH:13][C:8]([C:5]2[N:4]=[N:3][C:2]([Cl:1])=[CH:7][CH:6]=2)=[C:9]([OH:15])[CH:10]=1)[CH2:18][CH:17]=[CH2:16]Participants
3
Procedure
3-Chloro-6-(2,4-dihydroxyphenyl)pyridazine was reacted with but-3-enyl bromide under similar conditions to those described in Example 7a(i) to give 6-(4-but-3-enyloxy-2-hydroxyphenyl)-3-chloropyridazine.
Sources & evidence
- ORD record
- ord-d3d2f1097fe44999a16c514934adb8c9
- Source dataset
- uspto-grants-1977_10
- Patent number
- US04053601
Reaction notes
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