Hydrochloric Acid → HCID 9998921, compound

HRID 972819Notes

Reaction equation

HRID 972819 reaction equation
[NH2:1][CH:2]1[CH2:7][CH2:6][N:5]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH2:4][CH2:3]1.[N+:15]([C:18]1[CH:19]=[C:20]2[C:25](=O)[O:24][C:22](=[O:23])[C:21]2=[CH:27][CH:28]=1)([O-:17])=[O:16].Cl>>[CH2:8]([N:5]1[CH2:6][CH2:7][CH:2]([N:1]2[C:25](=[O:24])[C:20]3=[CH:19][C:18]([N+:15]([O-:17])=[O:16])=[CH:28][CH:27]=[C:21]3[C:22]2=[O:23])[CH2:3][CH2:4]1)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 2309764-Nitrophthalic acid anhydrideHCID 4158521-Benzyl-4-piperidylamine

Product 1

HCID 9998921HCID 9998921, compound

Procedure

9.51 Grams of 4-amino-1-benzylpiperidine and 9.66 grams of 4-nitrophthalic anhydride were reacted in a similar manner to that described in Example 14 to give 9.19 grams of the title compound as the monohydrochloride quarterhydrate. Melting Point: 240°-2° C.

Sources & evidence

ORD record
ord-53186ccf01fb41caa25b85d69e16158b
Source dataset
uspto-grants-1977_10
Patent number
US04053615

Reaction notes

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