HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl diethylphosphonocrotonate → Ethyl 5-(2-propyl-5-thiazolyl)2,4-pentadienoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl diethylphosphonocrotonate | HCID 7022350 | — |
| Reactant | 2-Propylthiazole-5-carbaldehyde | HCID 20369852 | — |
| Product | Ethyl 5-(2-propyl-5-thiazolyl)2,4-pentadienoate | HCID 54337588 | — |
Reaction Steps
Using the procedure of Example 4, 2-propyl-5-thiazole-carboxaldehyde [prepared by reaction of manganese dioxide and 2-propyl-5-hydroxymethyl-thiazole in benzene] and ethyl diethylphosphonocrotonate were reacted to obtain ethyl 5-(2-propyl-5-thiazolyl)-2,4-pentadienoate melting at 52°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04053618 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-f9c6658be54b4e6e9f4a074bf7c84924 |
| Source note | uspto-grants-1977_10 |