HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 972883Generated: October 26, 2026
Ethanolamine → 3-Methyl-4-phenylbut-3-enoic acid
https://huagongshe.com/reaction/972883
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | (3Z)-3-[(2E)-2-[1-[(E)-5,6-dimethylhept-3-en-2-yl]-7a-methyl-2,3,3a,5,6,7-hexahydro-1H-inden-4-ylidene]ethylidene]-4-methylcyclohexan-1-ol | HCID 5281010 | — |
| Reactant | HCID 54476880 | HCID 54476880 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 3-Methyl-4-phenylbut-3-enoic acid | HCID 293449 | — |
Reaction Steps
194 g of 3-methyl-4-phenyl-3-butenoic acid chloride (1 mole), dissolved into 500 ml benzene, are treated at-10° C with 183 g of monoethanolamine (3 moles). The mixture is stirred at 20° C for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04053635 |
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| Source dataset | uspto-grants-1977_10 |
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| ORD ID | ord-f85dc8370cbf44aea654c5a22599f515 |
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| Source note | uspto-grants-1977_10 |
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