1,2-Dichloroethane → HCID 178441982, compound

HRID 973047Notes

Reaction equation

HRID 973047 reaction equation
[C:1]([C:5]1[N:9]=[C:8]([SH:10])[NH:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2].[OH-].[K+].[Cl:13][CH2:14][CH2:15]Cl>>[Cl:13][CH2:14][CH2:15][S:10][C:8]1[NH:7][N:6]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[N:9]=1

Participants

4

Reactant 3

HCID 111,2-DichloroethaneHCID 14797Potassium HydroxideHCID 178441989HCID 178441989, compound

Product 1

HCID 178441982HCID 178441982, compound

Procedure

31.4 g. 3-t-Butyl-1,2,4-triazole-5-thiol was dissolved in 180 ml. industrial methylated spirits containing 12.4 g. potassium hydroxide. 99 g. 1,2-Dichloroethane was added and after four days the insoluble matter removed. 5-(2-Chloroethylthio)-3-t-butyl-1,2,4-triazole was obtained from the solution by evaporation.

Workup

  1. customremoved

Sources & evidence

ORD record
ord-3f3fdf4d514b4c11ae0d7e3ae89d921d
Source dataset
uspto-grants-1977_10
Patent number
US04054664

Reaction notes

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