Hydrochloric Acid → HCID 86735160, compound

HRID 973058Notes

Reaction equation

HRID 973058 reaction equation
[CH2:1]([O:13][C:14](=[O:21])[CH2:15][N:16]([CH2:18][CH:19]=[CH2:20])[CH3:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:22]>CO>[ClH:22].[CH2:1]([O:13][C:14](=[O:21])[CH2:15][N:16]([CH2:18][CH:19]=[CH2:20])[CH3:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21403442HCID 21403442, compound

Product 1

HCID 86735160HCID 86735160, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Two grams of N-allylsarcosine dodecyl ester was dissolved in 20 ml of methyl alcohol and 0.7 g of a 35% aqueous hydrochloric acid solution was gradually dropwise added thereto at room temperature with stirring. After reaction was completed, the methyl alcohol and water were removed under reduced pressure to obtain 2.2 g of the objective N-allylsarcosine dodecyl ester hydrochloride (m.p. 71° - 73° C).

Workup

  1. customAfter reaction
  2. customthe methyl alcohol and water were removed under reduced pressure

Sources & evidence

ORD record
ord-e74798e7d8b74fc7baa9d079c7a79edc
Source dataset
uspto-grants-1977_10
Patent number
US04054668

Reaction notes

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