HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 178440251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 178440243 | HCID 178440243 | — |
| Product | HCID 178440251 | HCID 178440251 | — |
Reaction Steps
220 g of 4,6-dihydroxy-2-isopropyl-pyrimidine are added at 0° C to 500 ml of 100% nitric acid and the mixture is stirred for 1 hour. Subsequently the nitration mixture is poured on ice water, filtered, washed with water, and dried in vacuo over P2O5, to yield 110 g of 4,6-dihydroxy-2-isopropyl-5-nitro-pyrimidine; m.p. 300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04055411 |
| Source dataset | uspto-grants-1977_10 |
| ORD ID | ord-e906395d1c9744f5b48f62a29e9a6279 |
| Source note | uspto-grants-1977_10 |