反应详情

100 mg of the compound from example 9 and 108 mg oxone were stirred in 2 ml MeOH at room temperature for 17 hrs. The mixture was filtered and the residue washed with THF. The combined filtrates were concentrated and purified by preparative HPLC-MS to yield 10 mg of the title compound.

1. filtrationThe mixture was filtered
2. washthe residue washed with THF
3. concentrationThe combined filtrates were concentrated
4. custompurified by preparative HPLC-MS