Hydrochloric Acid → HCID 21402677, compound

HRID 973252Notes

Reaction equation

HRID 973252 reaction equation
[C:1]1([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][CH2:9][C:10]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])=O)=[CH:3][CH:2]=1.Cl>>[C:1]1([C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)[CH:2]=[CH:3][C:4]([CH2:7][CH2:8][CH2:9][CH2:10][N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 21402676HCID 21402676, compound

Product 1

HCID 21402677HCID 21402677, compoundYield 63.8%

Procedure

4-(4-biphenylyl)-N,N-diethyl-butylamine was prepared by the procedure of Example IV except that 4-(4-biphenylyl)-N,N-diethyl-butyramide (b.p. 181.3° C. -- 10.05 mm) is also convertible to a non-toxic acid addition salt by reaction with a suitable acid such as hydrochloric acid. A yield of 63.8% was obtained having an m.p. of 133.4° C.

Workup

  1. customA yield of 63.8% was obtained

Sources & evidence

ORD record
ord-e009dc039bae48cdb7a2abc93020fb79
Source dataset
uspto-grants-1977_10
Patent number
US04055664

Reaction notes

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