HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitrobenzaldehyde → HCID 54105706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitrobenzaldehyde | HCID 72933 | — |
| Reactant | Propanedioic acid, monoethyl ester | HCID 3595298 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54105706 | HCID 54105706 | 31% |
Reaction Steps
33 g (250 millimoles) of monoethyl malonate and 27 g (150 millimoles) of 2-chloro-5-nitrobenzaldehyde in 100 ml of pyridine were reacted similarly to Example 1, and the mixture was worked up in a conventional manner. Yield: 31%, mp. 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05062884 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-70eac62e3ed940cfa02eb2dbb241bab6 |
| Source note | uspto-grants-1991_11 |