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HRID973378

反应详情

EQUATION

反应方程式

HRID 973378 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)CC(=O)O
HCID867

Propanedioic acid

C3H4O4

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：O=Cc1cc([N+](=O)[O-])ccc1Br
HCID11138942

2-Bromo-5-nitrobenzaldehyde

C7H4BrNO3

PRODUCTS

生成物

1
结构：O=C(O)C=Cc1cc([N+](=O)[O-])ccc1Br
HCID54106243

未命名化合物

收率 57%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

This reaction was carried out similarly to Example 1, with 2-bromo-5-nitrobenzaldehyde and malonic acid in pyridine and with piperidine. The product of melting point 185° C. was obtained in 57% yield.

WORKUP

后处理

  1. customThe product of melting point 185° C. was obtained in 57% yield