Phosphorus oxychloride → HCID 19988636, compound

HRID 973554Notes

Reaction equation

HRID 973554 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([C:9]2[N:14]=[CH:13][N:12]=[C:11](O)[CH:10]=2)[CH:6]=[CH:7][CH:8]=1)#[N:2].P(Cl)(Cl)([Cl:18])=O>>[Cl:18][C:11]1[CH:10]=[C:9]([C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([C:1]#[N:2])[CH:4]=2)[N:14]=[CH:13][N:12]=1

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 178509694HCID 178509694, compound

Product 1

HCID 19988636HCID 19988636, compound

Procedure

6-(3-cyanophenyl)-4-hydroxypyrimidine is boiled under reflux with phosphorus oxychloride to give the title compound.

Sources & evidence

ORD record
ord-b00acbf379d94b3e9df3e1dd1fa7eb33
Source dataset
uspto-grants-1991_11
Patent number
US05064832

Reaction notes

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