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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 973618Generated: October 30, 2026

Ammonia → HCID 19090926, compound

https://huagongshe.com/reaction/973618

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 19090879HCID 19090879—
CatalystNickelHCID 935—
SolventEthanolHCID 702—
ProductHCID 19090926HCID 19090926—

Reaction Steps

A mixture of 4,35 g of ethyl 2-cyanoethyl(di-n-propyloxymethyl)phosphinate, 10 g of ammonia and 2.3 g of Raney-Nickel in 170 ml of ethanol is hydrogenated for 10.5 hours. The catalyst is filtered off and the solvent is removed by evaporation. The crude oil is purified by distillation to yield ethyl 3-aminopropyl(di-n-propyloxymethyl)phosphinate as a colourless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05064819
Source datasetuspto-grants-1991_11
ORD IDord-d05c6116d4a4499c99bbd178414b334d
Source noteuspto-grants-1991_11