HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131717068, compound → HCID 178441824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131717068 | HCID 131717068 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178441824 | HCID 178441824 | — |
Reaction Steps
The title material can be prepared by treating a mixture of 4-(dimethylamino)-2 butyl 5-benzyloxycarbonyl-1-(2'-(N-triphenylmethyltetrazol-5-yl)biphen 4-yl)methylimidazole and 5 weight % of 10% Pd-C with H2 (at 40 psi) in EtOH for 16 hours, followed by filtration (Celite) and purification (SiO2 '35:65:1 CH2Cl2 /MeOH/NH4OH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064825 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-175d04fc1ab248f7b740feda2197e62a |
| Source note | uspto-grants-1991_11 |