Thionyl Chloride → HCID 14751482, compound

HRID 973716Notes

Reaction equation

HRID 973716 reaction equation
[CH:1]([C:5]1[C:10]([O:11][CH2:12][C:13](O)=[O:14])=[C:9]([Cl:16])[CH:8]=[C:7]([Cl:17])[CH:6]=1)([CH2:3][CH3:4])[CH3:2].S(Cl)([Cl:20])=O>>[CH:1]([C:5]1[C:10]([O:11][CH2:12][C:13]([Cl:20])=[O:14])=[C:9]([Cl:16])[CH:8]=[C:7]([Cl:17])[CH:6]=1)([CH2:3][CH3:4])[CH3:2]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 14751481HCID 14751481, compound

Product 1

HCID 14751482HCID 14751482, compound

Procedure

A mixture of 5.8 g of the product of Step C and 40 ml of thionyl chloride was refluxed for 2 hours and was evaporated to dryness under reduced pressure. The oil residue was washed with benzene and evaporated to dryness under reduced pressure to obtain 6.2 g of the desired product which was used as is for the next step.

Workup

  1. temperaturewas refluxed for 2 hours
  2. customwas evaporated to dryness under reduced pressure
  3. washThe oil residue was washed with benzene
  4. customevaporated to dryness under reduced pressure

Sources & evidence

ORD record
ord-9feeff11c4c448beb85e0d87e84673c0
Source dataset
uspto-grants-1991_11
Patent number
US05064861

Reaction notes

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