Thionyl Chloride → HCID 14751482, compound

Participants

Reaction Steps

A mixture of 5.8 g of the product of Step C and 40 ml of thionyl chloride was refluxed for 2 hours and was evaporated to dryness under reduced pressure. The oil residue was washed with benzene and evaporated to dryness under reduced pressure to obtain 6.2 g of the desired product which was used as is for the next step.

Provenance & Evidence