Hydrochloric Acid → HCID 19989034, compound

Participants

Reaction Steps

A mixture of 19.85 g of the product of Step B in 200 ml of ethanol and 38.1 ml of ethanolic 2N hydrogen chloride was refluxed with stirring for one hour and was then evaporated to dryness to obtain 18.67 g of raw product melting at 90° C. The product was crystallized from a refluxing mixture of 95-5 acetonitrile and water and was vacuum filtered. The product was empasted with isopropyl ether to obtain 8.44 g of the desired product melting at 160° C.

Provenance & Evidence