HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → [3-(Trifluoromethyl)phenoxy]acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-[3-(Trifluoromethyl)phenoxy]acetic acid | HCID 1991430 | — |
| Product | [3-(Trifluoromethyl)phenoxy]acetyl chloride | HCID 13140641 | — |
Reaction Steps
A solution of 6 g of the product of Step B in 36 ml of thionyl chloride was refluxed with stirring for one hour and was evaporated to dryness under reduced pressure to obtain 6.44 g of the desired product which was used as is for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064861 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-c09db5187a1f4a44a6e4420e23b35327 |
| Source note | uspto-grants-1991_11 |