HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178486068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | Tert-butyldicarbonate | HCID 22064466 | — |
| Reactant | HCID 178485225 | HCID 178485225 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178486068 | HCID 178486068 | 69.2% |
Reaction Steps
58.1 g of tert-butyl dicarbonate, 25.3 g of methyl thioisourea sulfate, 50 g of sodium bicarbonate, 500 ml of water and 500 ml of methylene chloride were stirred for 48 hours at 20° C. and after decanting, followed by extraction with methylene chloride and evaporation to dryness, 27 g of the expected product melting at 118° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064861 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-d3b96d5f31fd4049abe5ac4a9ae2cf38 |
| Source note | uspto-grants-1991_11 |