Thionyl Chloride → HCID 54116844, compound

HRID 973733Notes

Reaction equation

HRID 973733 reaction equation
[CH2:1]([C:4]1[C:14]([C:15]([F:18])([F:17])[F:16])=[CH:13][CH:12]=[CH:11][C:5]=1[O:6][CH2:7][C:8](O)=[O:9])[CH:2]=[CH2:3].S(Cl)([Cl:21])=O>>[CH2:1]([C:4]1[C:14]([C:15]([F:18])([F:17])[F:16])=[CH:13][CH:12]=[CH:11][C:5]=1[O:6][CH2:7][C:8]([Cl:21])=[O:9])[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 53999538HCID 53999538, compound

Product 1

HCID 54116844HCID 54116844, compound

Procedure

7 g of the product of Step D in 50 ml of thionyl chloride was refluxed for 2 hours and after concentrating, the residue was taken up in toluene. The solvents were eliminated under reduced pressure and the crude product obtained was used as is for Step F.

Workup

  1. concentrationafter concentrating

Sources & evidence

ORD record
ord-1c126dd3a32e4d5dbe17b403380c8260
Source dataset
uspto-grants-1991_11
Patent number
US05064861

Reaction notes

Loading…