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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 973733Generated: October 28, 2026

Thionyl Chloride → HCID 54116844, compound

https://huagongshe.com/reaction/973733

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 53999538HCID 53999538—
ProductHCID 54116844HCID 54116844—

Reaction Steps

7 g of the product of Step D in 50 ml of thionyl chloride was refluxed for 2 hours and after concentrating, the residue was taken up in toluene. The solvents were eliminated under reduced pressure and the crude product obtained was used as is for Step F.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05064861
Source datasetuspto-grants-1991_11
ORD IDord-1c126dd3a32e4d5dbe17b403380c8260
Source noteuspto-grants-1991_11