Hydrochloric Acid → HCID 53873723, compound

HRID 973734Notes

Reaction equation

HRID 973734 reaction equation
[CH2:1]([C:4]1[CH:16]=[CH:15][C:14]([C:17]([F:20])([F:19])[F:18])=[CH:13][C:5]=1[O:6][CH2:7][C:8]([O:10]CC)=[O:9])[CH:2]=[CH2:3].[OH-].[Na+].Cl>C(O)C>[CH2:1]([C:4]1[CH:16]=[CH:15][C:14]([C:17]([F:18])([F:19])[F:20])=[CH:13][C:5]=1[O:6][CH2:7][C:8]([OH:10])=[O:9])[CH:2]=[CH2:3]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 54149521HCID 54149521, compound

Product 1

HCID 53873723HCID 53873723, compoundYield 93.6%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Using the procedure of Step D of Example 16, 6.25 g of the product of Step A, 10.9 ml of 2N sodium hydroxide in 40 ml of ethanol were reacted and then 10.9 ml of 2N hydrochloric acid were added to obtain 5.28 g of the expected product.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-3a9ea91375dd49a18e5785c32c20b466
Source dataset
uspto-grants-1991_11
Patent number
US05064861

Reaction notes

Loading…