Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19989035 | HCID 19989035 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 54346887 | HCID 54346887 | — |
Reaction Steps
2.5 ml of ethyl bromoacetate were added to 4 g of the product of Step C in 15 ml of dimethylsulfoxide and 4 g of potassium carbonate were added, followed by heating at 80° C. for 2 hours 30 minutes. The reaction medium was poured into iced water and extracted with methylene chloride. The extracts were dried and concentrated to dryness to obtain 5.10 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05064861 |
|---|
| Source dataset | uspto-grants-1991_11 |
|---|
| ORD ID | ord-cc43f31632b04414a90af92024ee4d9e |
|---|
| Source note | uspto-grants-1991_11 |
|---|
