HuagongsheHuagongshe Chemistry Print Report · For research reference only
4H-Pyran-2-carboxylic acid, 5,6-dihydro-6,6-dimethyl-4-oxo- → HCID 15009971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4H-Pyran-2-carboxylic acid, 5,6-dihydro-6,6-dimethyl-4-oxo- | HCID 198592 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15009971 | HCID 15009971 | — |
Reaction Steps
In 8 ml of tetrahydrofuran was dissolved 0.5 g of 3,4-dihydro-2,2-dimethyl-4-oxo-2H-pyran-6-carboxylic acid, followed by adding thereto 50 mg of 10% palladium-carbon, and the reaction was carried out with stirring in a hydrogen stream at room temperature for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064945 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-67862387d6b3465395834ac03926fa24 |
| Source note | uspto-grants-1991_11 |