HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Trichloroacetonitrile | HCID 11011 | — |
| Reactant | Benzoic acid, 3-cyano-, methyl ester | HCID 83554 | — |
| Reactant | Bromhydrol | HCID 166749 | — |
| Product | Methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate | HCID 14572905 | — |
Reaction Steps
Methyl 3-cyanobenzoate (70 pw) are mixed with trichloroacetonitrile (376 pw) and aluminum bromide (13.9 pw) as described in Example 1, step 2, hydrogen chloride gas is added, the mixture is allowed to react and the reaction product is separated. Recrystallization from ethanol gives 160 pw=82% of white crystals of methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate. M.p.: 115 to 117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064959 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-75d789af17cf41cba765527cdb44a27a |
| Source note | uspto-grants-1991_11 |