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HRID973805

反应详情

EQUATION

反应方程式

HRID 973805 的结构方程式

REACTANTS

反应物

4
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：N#CC(Cl)(Cl)Cl
HCID11011

Trichloroacetonitrile

C2Cl3N

结构：COC(=O)c1cccc(C#N)c1
HCID83554

Benzoic acid, 3-cyano-, methyl ester

C9H7NO2

结构：[Al+3].[Br-].[Br-].[Br-]
HCID166749

Aluminum bromide (AlBr3)

AlBr3

PRODUCTS

生成物

1
结构：COC(=O)c1cccc(-c2nc(C(Cl)(Cl)Cl)nc(C(Cl)(Cl)Cl)n2)c1
HCID14572905

未命名化合物

PROCEDURE

实验过程

Methyl 3-cyanobenzoate (70 pw) are mixed with trichloroacetonitrile (376 pw) and aluminum bromide (13.9 pw) as described in Example 1, step 2, hydrogen chloride gas is added, the mixture is allowed to react and the reaction product is separated. Recrystallization from ethanol gives 160 pw=82% of white crystals of methyl 3-(4,6-bis(trichloromethyl)-s-triazin-2-yl)benzoate. M.p.: 115 to 117° C.

WORKUP

后处理

  1. additionis added
  2. customto react
  3. customthe reaction product is separated
  4. customRecrystallization from ethanol