HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 178429185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | 5-amino-1H-1,2,4-triazole-3-thiol | HCID 178509296 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178429185 | HCID 178429185 | 37.6% |
Reaction Steps
A mixture of 3-amino-5-mercapto-s-triazole (10 g), ethyl acetoacetate (34 g), piperidine (10 ml) and ethanol (300 ml) was refluxed for four hours. After removing the solvent by distillation under reduced pressure, 150 ml water was added, the mixture was neutralized to pH 7.0 with hydrochloric acid and cooled, giving 5.9 g of the objective compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064953 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-da9e5a02aec943218c6689899b198de5 |
| Source note | uspto-grants-1991_11 |