Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → HCID 178524623, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | HCID 178498582 | HCID 178498582 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178524623 | HCID 178524623 | 92.4% |
반응 단계
The product obtained in Step 1 (4.5 g) was added to a solution of 1.7 g potassium hydroxide in 50 ml water, and the mixture was refluxed for two hours. After cooling to room temperature, the solution was washed with 50 ml of ethyl acetate, the pH was adjusted to 1.0 with hydrochloric acid, and the formed crystals were collected by filtration, affording 3.9 g of the objective compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05064953 |
| 출처 데이터셋 | uspto-grants-1991_11 |
| ORD ID | ord-8ad0b0fb11e644bc8cd3e5b70784d2c8 |
| 출처 메모 | uspto-grants-1991_11 |