HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178428721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 178429730 | HCID 178429730 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178428721 | HCID 178428721 | — |
Reaction Steps
Hydrazine monohydrate (6.4 ml) was added dropwise to a suspension of 2,4-dimercapto-6-methylpyrimidine (7.0 g) in 100 ml of ethanol at room temperature, the mixture was refluxed for two hours, and the crystals formed upon cooling were collected by filtration and washed with 100 ml of ethanol, giving 6.4 g of the objective compound as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05064953 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-c215d61e5bdb4b6f8f7e4f210f865be2 |
| Source note | uspto-grants-1991_11 |