Hydrazine hydrate (1:1) → HCID 178428721, compound

HRID 973856Notes

Reaction equation

HRID 973856 reaction equation
O.[NH2:2][NH2:3].[SH:4][C:5]1[N:10]=[C:9](S)[CH:8]=[C:7]([CH3:12])[N:6]=1>C(O)C>[NH:2]([C:9]1[CH:8]=[C:7]([CH3:12])[N:6]=[C:5]([SH:4])[N:10]=1)[NH2:3]

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 178429730HCID 178429730, compound

Product 1

HCID 178428721HCID 178428721, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Hydrazine monohydrate (6.4 ml) was added dropwise to a suspension of 2,4-dimercapto-6-methylpyrimidine (7.0 g) in 100 ml of ethanol at room temperature, the mixture was refluxed for two hours, and the crystals formed upon cooling were collected by filtration and washed with 100 ml of ethanol, giving 6.4 g of the objective compound as yellow crystals.

Workup

  1. temperaturethe mixture was refluxed for two hours
  2. customthe crystals formed
  3. temperatureupon cooling
  4. filtrationwere collected by filtration
  5. washwashed with 100 ml of ethanol

Sources & evidence

ORD record
ord-c215d61e5bdb4b6f8f7e4f210f865be2
Source dataset
uspto-grants-1991_11
Patent number
US05064953

Reaction notes

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