HCID 178441397, compound → HCID 178441392, compound

HRID 973883Notes

Reaction equation

HRID 973883 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][CH:5]1[C:40](=[O:41])[O:39][CH:38]([CH:42]([CH:44]([OH:52])[CH2:45][CH2:46][CH2:47][NH:48][C:49]([NH2:51])=[NH:50])[CH3:43])[CH:37]([CH3:53])[CH:36]=[C:35]([CH3:54])[CH2:34][CH2:33][CH2:32][CH2:31][CH:30]([OH:55])[CH2:29][CH:28]([OH:56])[CH2:27][CH:26]([OH:57])[CH2:25][CH:24]([OH:58])[CH2:23][CH:22]([OH:59])[CH:21]([O:60][C@H:61]2[O:65][C@H:64]([CH2:66][OH:67])[C@@H:63]([OH:68])[C@@H:62]2[OH:69])[CH:20]=[C:19]([CH3:70])[CH:18]([OH:71])[CH2:17][CH2:16][CH2:15][CH:14]([OH:72])[CH2:13][CH2:12][CH2:11][CH:10]([OH:73])[CH2:9][CH2:8][CH:7]([CH3:74])[CH:6]1[OH:75].CN1C(=O)CCC1>CN(C)C(=O)C>[CH3:1][CH2:2][CH2:3][CH2:4][CH:5]1[C:40](=[O:41])[O:39][CH:38]([CH:42]([CH:44]([OH:52])[CH2:45][CH2:46][CH2:47][NH:48][C:49]([NH2:51])=[NH:50])[CH3:43])[CH:37]([CH3:53])[CH:36]=[C:35]([CH3:54])[CH2:34][CH2:33][CH2:32][CH2:31][CH:30]([OH:55])[CH2:29][CH:28]([OH:56])[CH2:27][CH:26]([OH:57])[CH2:25][CH:24]([OH:58])[CH2:23][CH:22]([OH:59])[CH:21]([O:60][C@H:61]2[O:65][C@H:64]([CH2:66][OH:67])[C@@H:63]([OH:68])[C@@H:62]2[OH:69])[CH:20]=[C:19]([CH3:70])[CH:18]([OH:71])[CH2:17][CH2:16][CH2:15][CH:14]([OH:72])[CH2:13][CH2:12][CH2:11][CH:10]([OH:73])[CH2:9][CH2:8][CH:7]([CH3:74])[CH:6]1[OH:75]

Participants

3

Reactant 1

HCID 178441397HCID 178441397, compound

Product 1

HCID 178441392HCID 178441392, compound

Reagents, catalysts & solvents 1

HCID 31374DimethylacetamideSolvent

Procedure

The primycin-NMP basic gel is dissolved in N,N-dimethyl-acetamide under warming and the warm solution is sprayed onto a zinc oxide-talc powder mixture prepared according to Example 15. The sprayed powder mixture is kept in an essiccator for 24 hours at 40° C. and sieved (sieve No. VI, mesh 0.16 mm) and finally homogenized. Thus a white homogeneous powder mixture is obtained.

Workup

  1. temperatureunder warming
  2. customprepared
  3. filtrationsieved (sieve No
  4. customThus a white homogeneous powder mixture is obtained

Sources & evidence

ORD record
ord-99c5ac6e8fd94bccb61c9d0be02586e3
Source dataset
uspto-grants-1991_11
Patent number
US05064815

Reaction notes

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