HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14479947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | HCID 22718852 | HCID 22718852 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14479947 | HCID 14479947 | — |
Reaction Steps
A mixture of 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (1.19 g, 5 mmole), N-benzyl-N-isopropyl-2-propenamide (1.0 g, 5 mmole) (prepared from acryloyl chloride and benzylisopropylamine), and triethylamine (0.05 ml) in methanol was stirred for 60 hours at room temperature. The reaction mixture was concentrated in vacuo to an oil. Chromatography on silica gel gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05066679 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-7a7aac450e104d1b95f5f0552a1b2b96 |
| Source note | uspto-grants-1991_11 |