HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 15675485, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Methylhydroxylamine | HCID 11647 | — |
| Reactant | HCID 17131188 | HCID 17131188 | — |
| Product | HCID 15675485 | HCID 15675485 | — |
Reaction Steps
This hydrochloride was converted to the title compound by treatment with phosgene and N-methylhydroxylamine as in Example 32 above. Recrystallization from methanol-water provided a white powder (0.46 g, 25% yield), mp 178°-179° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05066658 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-13983080390d40d88ea15a5fe6d79a75 |
| Source note | uspto-grants-1991_11 |