HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → 3-[(2-phenylethyl)amino]propanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[(2-phenylethyl)amino]propanenitrile | HCID 3155309 | — |
Reaction Steps
5.3 g of acrylonitrile are added dropwise to a solution of 12.1 g of N-benzylmethylamine in 20 ml of ethanol. The reaction mixture is stirred for three hours at room temperature and then concentrated under vacuum to give 17 g (Y=97%) of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068064 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-9603e5dde5fc48b2bca3abb3095c79f5 |
| Source note | uspto-grants-1991_11 |