Hydrochloric Acid → HCID 54375921, compound

HRID 974288Notes

Reaction equation

HRID 974288 reaction equation
C([NH:4][C:5]1[S:6][C:7]2[CH2:8][CH2:9][N:10]([CH2:15][CH:16]=[CH:17][C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=3)[CH2:11][CH2:12][C:13]=2[N:14]=1)(=O)C.Cl>>[NH2:4][C:5]1[S:6][C:7]2[CH2:8][CH2:9][N:10]([CH2:15][CH:16]=[CH:17][C:18]3[CH:19]=[CH:20][C:21]([Cl:24])=[CH:22][CH:23]=3)[CH2:11][CH2:12][C:13]=2[N:14]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 54337104HCID 54337104, compound

Product 1

HCID 54375921HCID 54375921, compoundYield 71%

Procedure

Prepared from 2-acetylamino-6-(3-(4-chloro-phenyl)allyl)-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine with semi-concentrated hydrochloric acid. Yield: 71% of theory, Melting point: 145°-150° C.

Sources & evidence

ORD record
ord-9eba1c41fb7b401385ea2d69a673aa0d
Source dataset
uspto-grants-1991_11
Patent number
US05068325

Reaction notes

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