HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 53675793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 54508890 | HCID 54508890 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 53675793 | HCID 53675793 | 10% |
Reaction Steps
Prepared from 4-methoxy-cinnamyl chloride and 1 equivalent of 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine in the presence of 1 equivalent of potassium carbonate in chloroform. Yield: 10% of theory, Melting point: 155-160° C. (ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-560bef6e872946eebcb3b833a4978577 |
| Source note | uspto-grants-1991_11 |