HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 54500731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-Amino-4,5,6,7,8-pentahydrothiazolo[5,4-d]azepine | HCID 19985785 | — |
| Reactant | HCID 53741517 | HCID 53741517 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54500731 | HCID 54500731 | 52% |
Reaction Steps
Prepared from 2-methyl-cinnamyl chloride and 2 equivalents of 2-amino-4,5,7,8-tetrahydro-6H-thiazolo[5,4-d]azepine in chloroform. Yield: 52% of theory, Melting point: 112°-115° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05068325 |
| Source dataset | uspto-grants-1991_11 |
| ORD ID | ord-fc7e5938a8054ce7ab10d0076d229040 |
| Source note | uspto-grants-1991_11 |